CERTIFICATE OF ANALYSIS

PRODUCT NAME: N-Boc Linagliptin
Date of Mfg: Sample COA RETEST DATE: Sample COA
Catalogue Number LIG-012
Lot Number Sample COA
Batch Quantity Sample COA
CAS Number 668273-75-4
Mol. Formula C₃₀H₃₆N₈O₄
Molecular Wt 572.66
Long Term Storage Condition 2-8°C Refrigerator Handling instruction Sample COA
IUPAC tert-butyl N-[(3R)-1-[7-but-2-ynyl-3-methyl-1-[(4-methylquinazolin-2-yl)methyl]-2,6-dioxopurin-8-yl]piperidin-3-yl]carbamate
Chemical Name N-Boc Linagliptin
Synonyms Linagliptin Related Compound B, N-[(3R)-1-[7-(2-butyn-1-yl)-2,3,6,7-tetrahydro-3-methyl-1-[(4-methyl-2-quinazolinyl)methyl]-2,6-dioxo-1H-purin-8-yl]-3-piperidinyl]-carbamic Acid 1,1-Dimethylethyl Ester
Test Results
Appearance Off-White to Pale Beige Solid
Identification by 1H NMR Sample COA
Identification By IR Sample COA
Mass (ESI) Sample COA
Purity 97% BY HPLC
Wt. Loss by TGA Sample COA
% Potency Sample COA
Solubility Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
QC Release Date Sample COA
Attachments Sample COA
Note: This material can be used as a referance standard and is for research purpose ONLY and not for human consumption
This is Sample COA