CERTIFICATE OF ANALYSIS

PRODUCT NAME: Linagliptin Impurity 32
Date of Mfg: Sample COA RETEST DATE: Sample COA
Catalogue Number LIG-011
Lot Number Sample COA
Batch Quantity Sample COA
CAS Number 853029-57-9
Mol. Formula C₂₀H₁₇BrN₆O₂
Molecular Wt 453.29
Long Term Storage Condition Store under 2 to 8°C Handling instruction Sample COA
IUPAC 8-bromo-7-but-2-ynyl-3-methyl-1-[(4-methylquinazolin-2-yl)methyl]purine-2,6-dione
Chemical Name Linagliptin Impurity 32
Synonyms 1-[(4-Methylquinazolin-2-yl)methyl]-3-methyl-7-(2-butyn-1-yl)-8-bromoxanthine
Test Results
Appearance White to Pale Yellow Solid
Identification by 1H NMR Sample COA
Identification By IR Sample COA
Mass (ESI) Sample COA
Purity NLT 98% BY HPLC
Wt. Loss by TGA Sample COA
% Potency Sample COA
Solubility DMSO (Slightly, Heated, Sonicated), Methanol (Very Slightly, Heated, Sonicated)
QC Release Date Sample COA
Attachments Sample COA
Note: This material can be used as a referance standard and is for research purpose ONLY and not for human consumption
This is Sample COA