PRODUCT NAME: Linagliptin N-Acetyl Impurity
Date of Mfg: Sample COA	RETEST DATE: Sample COA

Catalogue Number	LIG-021
Lot Number	Sample COA
Batch Quantity	Sample COA
CAS Number	1803079-49-3
Mol. Formula	C27H30N8O3
Molecular Wt	514.58 g/mol
Long Term Storage Condition	2-8°C Refrigerator	Handling instruction	Sample COA
IUPAC	((R)-N-(1-(7-(but-2-yn-1-yl)-3-methyl-1-((4-methylquinazolin-2-yl)methyl)-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)piperidin-3-yl)acetamide)
Chemical Name	Linagliptin N-Acetyl Impurity
Synonyms	Linagliptin Acetamide; 8-[(3R)-3-Acetylamino-1-piperidinyl]-7-(2-butyn-1-yl)-3,7-dihydro-3-methyl-1-[(4-methyl-2-quinazolinyl)methyl]-1H-purine-2,6-dione; (R)-N-(1-(7-(But-2-yn-1-yl)-3-methyl-1-((4-methylquinazolin-2-yl)methyl)-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)piperidin-3-yl)acetamide

Test	Results
Appearance	Light Yellow Solid
Identification by 1H NMR	Sample COA
Identification By IR	Sample COA
Mass (ESI)	Sample COA
Purity	NLT 98%
Wt. Loss by TGA	Sample COA
% Potency	Sample COA
Solubility
QC Release Date	Sample COA
Attachments	Sample COA
Note: This material can be used as a referance standard and is for research purpose ONLY and not for human consumption