PRODUCT NAME: Alogliptin Impurity 22
Date of Mfg: Sample COA	RETEST DATE: Sample COA

Catalogue Number	ALP-024
Item/Batch Number	Sample COA
Quantity	Sample COA
CAS Number	655-63-0
Mol. Formula	C8H5Br2N
Molecular Wt	274.9 g/mol
IUPAC	2-(Dibromomethyl)benzonitrile
Synonyms	o-Cyanobenzal bromide; o-Cyanobezylidene Bromide
Long Term Storage Condition	Store in a cool, dry, and well-ventilated place
Handling instruction	Sample COA

Test	Results
Appearance	off-white to light beige or tan crystalline powder
Water content by KF/TGA	Sample COA
% Potency = [100 - (Water content by KF)] X HPLC Purity)] / 100	Sample COA
Identification by HNMR	Sample COA
Identification By IR	Sample COA
Mass (ESI)	Sample COA
Solubility
Purity	NLT 98%
Analysis Date (Release Date)	Sample COA
Attachments	Sample COA
Other Information	Sample COA
Note: This material can be used as a referance standard and is for research purpose ONLY and not for human consumption