CERTIFICATE OF ANALYSIS

PRODUCT NAME: Vildagliptin Amide Impurity
Date of Mfg: Sample COA RETEST DATE: Sample COA
Catalogue Number VIL-012
Lot Number Sample COA
Batch Quantity Sample COA
CAS Number 565453-39-6
Mol. Formula C₁₇H₂₇N₃O₃
Molecular Wt 321.41
Long Term Storage Condition Refrigerator, under inert atmosphere Handling instruction Sample COA
IUPAC 1-[2-[(3-hydroxy-1-adamantyl)amino]acetyl]pyrrolidine-2-carboxamide
Chemical Name Vildagliptin Amide Impurity
Synonyms Vildagliptin Impurity A;N-(3-Hydroxytricyclo[3.3.1.13,7]dec-1-yl)glycyl-L-prolinamide
Test Results
Appearance White to Off-White Solid
Identification by 1H NMR Sample COA
Identification By IR Sample COA
Mass (ESI) Sample COA
Purity NLT 98%
Wt. Loss by TGA Sample COA
% Potency Sample COA
Solubility Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
QC Release Date Sample COA
Attachments Sample COA
Note: This material can be used as a referance standard and is for research purpose ONLY and not for human consumption
This is Sample COA